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IR and X-ray time-resolved simultaneous experiments: an opportunity to investigate the dynamics of complex systems and non-equilibrium phenomena using third-generation synchrotron radiation sources

Marcelli, Augusto Claudio and Innocenzi, Plinio and Malfatti, Luca and Newton, Mark A. and Rau, Julietta V. and Ritter, Eglof and Schade, Ulrich and Xu, Wei (2012) IR and X-ray time-resolved simultaneous experiments: an opportunity to investigate the dynamics of complex systems and non-equilibrium phenomena using third-generation synchrotron radiation sources. Journal of Synchrotron Radiation, Vol. 19 (6), p. 892-904. ISSN 0909-0495. eISSN 1600-5775. Article.

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DOI: 10.1107/S0909049512041106

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Abstract

Third-generation storage rings are modern facilities working with high currents and designed to host powerful radiation sources, like undulators and wigglers, and to deliver high-brilliance beams to users. Many experiments at high spatial resolution, such as spectromicroscopy at the nanometre scale and with high temporal resolution to investigate kinetics down to the picosecond regime, are now possible. The next frontier is certainly the combination of different methods in a unique set-up with the ultimate available spatial and temporal resolutions. In the last decade much synchrotron-based research has exploited the advantage of complementary information provided by time-resolved X-ray techniques and optical methods in the UV/Vis and IR domains. New time-resolved and concurrent approaches are necessary to characterize complex systems where physical–chemical phenomena occur under the same experimental conditions, for example to detect kinetic intermediates via complementary but independent observations. In this contribution we present scientific cases from original works and literature reviews to support the proposed IR/X-ray simultaneous approach, with both probes exploiting synchrotron radiation sources. In addition, simple experimental layouts that may take advantage of the high brilliance and the wide spectral distribution of the synchrotron radiation emission will be given for specific researches or applications to investigate dynamic processes and nonequilibrium phenomena occurring in many condensed matter and biological systems, of great interest for both fundamental research and technological applications.

Item Type:Article
ID Code:8116
Status:Published
Refereed:Yes
Uncontrolled Keywords:X-ray, infrared, time-resolved spectroscopy
Subjects:Area 09 - Ingegneria industriale e dell'informazione > ING-IND/22 Scienza e tecnologia dei materiali
Divisions:001 Università di Sassari > 01-a Nuovi Dipartimenti dal 2012 > Architettura, Design e Urbanistica
001 Università di Sassari > 01 Dipartimenti > Architettura e pianificazione > LMNT-Laboratorio di Scienza dei Materiali e NanoTecnologie
Publisher:Blackwell / Wiley
ISSN:0909-0495
eISSN:1600-5775
Copyright Holders:© International Union of Crystallography
Additional Information:Presented at the International workshop on "Improving Data Quality and Quantity for XAFS experiments" (Q2XAFS2011), Tsukuba, Japan, 8-9 December 2011.
Deposited On:08 Nov 2012 09:05

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