D'Antona, Nicola and Morrone, Raffaele and Bovicelli, Paolo and Gambera, Giovanni and Kubáč, David and Martínková, Ludmila (2010) A Novel chemo-multienzymatic synthesis of bioactive cyclophellitol and epi-cyclophellitol in both enantiopure forms. Tetrahedron: Asymmetry, Vol. 21 (20), p. 2448-2454. eISSN 1362-511X. Article.
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A new route to synthesize cyclophellitol and epi-cyclophellitol from racemic starting materials in enantiopure forms has been developed. The synthesis involves a multi-enzymatic biotransformation pathway of the novel cyano-cyclitol (1R,4S,5R,6R)/(1S,4R,5S,6S)-4,5,6-trihydroxycyclohex-2-enecarbonitrile by a cooperative use of lipase, nitrile hydratase, and amidase.
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