Palombi, Laura and Bocchino, Carmen and Caruso, Tonino and Villano, Rosaria and Scettri, Arrigo (2008) Cathodic C-H electro-activation in ionic liquid: an improved electrochemical method for the conjugate addition of 1,3-dicarbonyl compounds. Catalysis Communications, Vol. 10 (3), p. 321-324. ISSN 1566-7367. Article.
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The constant current electrolysis of 1,3-dicarbonyl compounds in 1-ethyl-3-methylimidazolium ethylsulfate (EMIMEtSO4) ionic liquid provided the direct deprotonation of the methylene active functionality to the cathode: the corresponding enolates efficiently underwent to the one-pot Michael addition with activated olefins.
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